A chlorine-free protocol for processing germanium
General conditions: 3 (250 mg), RMgCl (20 equiv), THF (10 ml), 65°C for 24 hours. a Complex 4 used in place of complex 3. b Complex 5 used in place of complex 3. c Using MeMgBr in Bu 2 O; 1 H NMR yield using toluene as an internal standard. d Isolated as a 10:1 mixture with bibenzyl.
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